November 2015 Archives

#220 Methods of Thickness Test for Plate Coating

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When you place or receive an order of plate coating work, the thickness of the plating film is probably the most important specifications. The plating type and thickness are determined by the operating environment and purposes of the particular product. This section explains how to measure the thickness of plate coatings.

(1) Methods of the thickness test

JIS provides the following methods to test the thickness of plate coatings:

No.Measurement methodAccuracyDescription of the method
1Microscopical exam of cross section0.8umPrepare a cross-section sample of the plating surface. Measure the thickness by enlarging it by a microscope.
2Coulometric methodWithin 10% from the true value in the range of 0.2 to 50umSet the electrolysis equipment on the plating surface. Dissolve the metallic plating film by electrolysis and measure the thickness.
3Eddy current methodAround 10% from the true valuePlace a probe supplying high-frequency current on the plating surface and read the plating thickness directly.
4Magnetic methodWithin 10% from the true value excluding the thin film of 5um or lessPlace a probe emitting lines of magnetic force on the plating surface and read the plating thickness directly.
5X-ray spectrometric methodWithin 10% from the true valueIrradiate X-ray on the plating surface. Measure the plating thickness by the intensity of fluorescent X-ray generated.
6Beta backscatter methodWithin 10% from the true valueIrradiate beta ray on the plating surface. Directly read the plating thickness from the back-scattered volume.
7Micrometer test methodUse a micrometer or a dial gauge to measure the plating thickness based on the dimensional difference before and after the plating work.
8Coating weight measurement by gravimetric methodPeel off the sample plating of a specified area. Based on the weight difference before and after this process, calculate the adhesion amount per unit area.

(2) Sampling method

 1.  In general, collect a sample from the significant surface of the plated goods. If it is not possible, substitute the significant surface of the plated goods with a test piece made of the same materials and created in the same conditions as the subject goods.
 2.  The sample surface must be clean. If any dust or oil content was found on the surface, remove them without damaging the plated surface before performing the test.

#219 Metal Cleaning Method - 2

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(3) Cleaning with solvents

This is a solvent degreasing method that has been in use since the old times.In the past, trichloroethylene (TCE) and perchlorethylene (PCE) were used for this purpose. However, their use and production have been banned due to their toxicity.Currently, the following types of solvent are used for metal cleaning:

(1) Aliphatic hydrocarbon --- Petroleum solvent
(2) Aromatic hydrocarbon --- Coal tar solvent
(3) Non-combustible solvent --- Chlorinated hydrocarbon
(4) Polar solvent --- Ketone, Alcohol, and Phenol

These solvents are processed by a dedicated solvent degreaser and used in the following forms: vapor degreasing, liquid degreasing, and a combination of both as the most common method.(See [Fig.1]) First, clean a room-temperature workpiece in the vapor-phase tank filled with solvent vapor. As the temperature rises up to the steam temperature, cool it off with the room-temperature solvent. Then, heat up and dry the workpiece in the vapor-phase tank.

Figure

(5) Special solution --- Emulsifying solvent, biphasic solvent, emulsion cleaner

These types of solution are used in the liquid form (aqueous solution) for immersion degreasing.

(4) Cleaning by chemical reactions

This method includes acid pickling and alkaline rust removal.Fill a dedicated tank with solution. Soak the product in that tank to remove rust and activate the metal surface.There is also a method using an electrolytic action together.

(1) Acids --- Make the oxides/sulfides soluble using hydrochloric acid and sulfuric acid, etc.
(2) Alkalis --- Alkaline salt and complex salt-forming agent (gluconic acid, thioglycolic acid salt, etc.)

(5) Mechanical cleaning method

(1) Wiping --- Use emery cloth or non-woven fabric (Scotch Brite™) and wipe it off with hand.
(2) Polishing and machining --- The most common method is buffing. Finish the surface as desired.([Fig.2])
(3) Blasting --- Use abrasive materials such as silica sand, steel grit, or glass beads to create a satin finish.
(4) Blasting by water/air --- Use alumina or silicon carbide to make the surface smoother than (3).

Figure

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